1: n-dodecanol With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 Angstroem MS in dichloromethane
2: (ethyl)-triphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; hexane; dichloromethane
T=-78 - 20°C; Wittig olefination;
参考文献
MacCoss, Rachel N.; Balskus, Emily P.; Ley, Steven V.
Tetrahedron Letters, 2003 , vol. 44, # 42 p. 7779 - 7781
1: (ethyl)-triphenylphosphonium bromide With potassium tert-butylate in tetrahydrofuran
T=20°C; Wittig Olefination; 0.0833333 h;
2: 2-methyl-benzaldehyde in tetrahydrofuran
Wittig Olefination;
参考文献
Baccolini, Graziano; Delpivo, Camilla; Micheletti, Gabriele
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 11 p. 1291 - 1302
1: (ethyl)-triphenylphosphonium bromide With potassium tert-butylate in tetrahydrofuran
T=20°C; Wittig Olefination; 0.0833333 h;
2: pentanal in tetrahydrofuran
Wittig Olefination;
参考文献
Baccolini, Graziano; Delpivo, Camilla; Micheletti, Gabriele
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 11 p. 1291 - 1302
