2-(烯丙氧基)-5-氯苯甲醛合成路线 （共 5 条）
反应条件
sodium hydroxide; (benzyl)-tri-(butyl)-ammonium chloride in dichloromethane Ambient temperature;
参考文献
Lee, Jong In; Lee, Hyo San; Kim, Byeang Hyean
Synthetic Communications, 1996 , vol. 26, # 17 p. 3201 - 3215
反应条件
1: CH2Cl2 2: 60 percent / 650 °C / 0 - 0.01 Torr View Scheme
参考文献
Black, Michael; Cadogan, J. I. G.; Cartwright, Gary A.; McNab, Hamish; MacPherson, Andrew D.
Journal of the Chemical Society, Chemical Communications, 1993 , # 11 p. 959 - 960
反应条件
1: zinc / N,N-dimethyl-formamide; tetrahydrofuran / 20 °C
2: Jone's reagent / acetone / 0 °C
3: silver nitrate / acetonitrile / 1.5 h / 80 °C
4: water / 60 - 150 °C / |Microwave irradiation
5: dihydrogen peroxide / water; ethanol / 40 - 80 °C / |Microwave irradiation
View Scheme
参考文献
He, Yan; Zhang, Xinying; Cui, Liangyan; Wang, Jianji; Fan, Xuesen
Green Chemistry, 2012 , vol. 14, # 12 p. 3429 - 3435
反应条件
1: CH2Cl2
2: 85 percent / 650 °C / 0 - 0.01 Torr
View Scheme
参考文献
Black, Michael; Cadogan, J. I. G.; Cartwright, Gary A.; McNab, Hamish; MacPherson, Andrew D.
Journal of the Chemical Society, Chemical Communications, 1993 , # 11 p. 959 - 960
反应条件
3-(2,4,6-trimethyl-phenyl)-5,6,7,8-tetrahydro-4H-cycloheptathiazol-3-ium perchlorate; 1,8-diazabicyclo[5.4.0]undec-7-ene in 1,4-dioxane
T=120°C; 2 h; Inert atmosphere;
参考文献
Hirano, Keiichi; Biju, Akkattu T.; Piel, Isabel; Glorius, Frank
Journal of the American Chemical Society, 2009 , vol. 131, # 40 p. 14190 - 14191
