2-(1-苯乙烯基)吡啶合成路线 （共 23 条）
反应条件
hydrogen; [Rh(1,3-dimesitylimidazole-2-ylidene)(cod)Cl] in toluene T=125°C; 24 h;
参考文献
Ahmed, Moballigh; Buch, Cathleen; Routaboul, Lucie; Jackstell, Ralf; Klein, Holger; Spannenberg, Anke; Beller, Matthias
Chemistry - A European Journal, 2007 , vol. 13, # 5 p. 1594 - 1601
反应条件
1: 85 percent / Na / 6 h / 20 °C 2: aq. potassium tert-butoxide / diethyl ether / 25 °C 3: 80 percent / tetrabutylammonium periodate / dioxane / 20 h / Heating 4: 100 percent / H2 / PtO2 / toluene / 12 h / 120 °C / 38000 Torr View Scheme
参考文献
Marchetti, Mauro; Sechi, Barbara; Azzena, Ugo; Botteghi, Carlo; Paganelli, Stefano; Ponte, Gino Del; Stefani, Helio A.
Anales de Quimica, 1998 , vol. 94, # 4-5 p. 219 - 225
反应条件
sulfuric acid
T=100°C; 0.25 h;
参考文献
Rennison, David; Bova, Sergio; Cavalli, Maurizio; Ricchelli, Fernanda; Zulian, Alessandra; Hopkins, Brian; Brimble, Margaret A.
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 8 p. 2963 - 2974
反应条件
triphenyl-arsane; bis(dibenzylideneacetone)-palladium(0) in toluene
T=110°C;
参考文献
Chen, Shu-Hui
Tetrahedron Letters, 1997 , vol. 38, # 27 p. 4741 - 4744
反应条件
tetrabutylammomium bromide; potassium carbonate; bis-lt;(4-Cl-2-PdCl-Ph)-(4-Cl-Ph)-methanone oximegt; in 1-methyl-pyrrolidin-2-one
T=160°C; Heck-Mizoroki-Jeffery reaction; 30 h;
参考文献
Alonso, Diego A.; Najera, Carmen; Pacheco, Ma. Carmen
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 2 p. 172 - 183
反应条件
in tetrahydrofuran
T=25°C;
参考文献
Ukai; Arioka; Yoshino; Fushimi; Oshima; Utimoto; Matsubara
Synlett, 2001 , # 4 p. 513 - 514
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in ethanol; toluene
Suzuki coupling; 5 h; Inert atmosphereReflux;
参考文献
Nunez, Ana; Abarca, Beatriz; Cuadro, Ana M.; Alvarez-Builla, Julio; Vaquero, Juan J.
Journal of Organic Chemistry, 2009 , vol. 74, # 11 p. 4166 - 4176
反应条件
sodium peroxodisulphate; N-n-hexyl-N-methylamine
T=120°C; 4 h;
参考文献
Itoh, Masaki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2014 , vol. 16, # 7 p. 2050 - 2053
反应条件
anhydrous magnesium perchlorate; NADH model 2 in acetonitrile
T=60°C;
参考文献
Levacher, Vincent; Valque, Claude; Coupa, Sophie; Dupas, Georges; Queguiner, Guy; Bourguignon, Jean
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 4 p. 1211 - 1215
反应条件
sodium peroxodisulphate; copper (II) acetate monohydrate
T=120°C; 0.5 h; Inert atmosphere;
参考文献
Itoh, Masaki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2014 , vol. 16, # 7 p. 2050 - 2053
