3-(2,2,2-三氟乙氧基)-1-丙烯合成路线 (共 13 条)
反应条件
1: 2,2,2-trifluoroethanol With potassium hydroxide T=20°C; 1 h; 2: allyl bromide in water T=0°C;
参考文献
Audouard, Christophe; Garayt, Maxime R.; Kerouredan, Erwan; Percy, Jonathan M.; Yang, Hongli
Journal of Fluorine Chemistry, 2005 , vol. 126, # 4 p. 611 - 623
反应条件
potassium hydroxide in water T=40°C; 18 h;
参考文献
Audouard, Christophe; Fawcett, John; Griffith, Gerry A.; Kerouredan, Erwan; Miah, Afjal; Percy, Jonathan M.; Yang, Hongli
Organic Letters, 2004 , vol. 6, # 23 p. 4269 - 4272
反应条件
in dimethyl sulfoxide T=10 - 20°C; Etherification; 12 h;
参考文献
Omotowa, Bamidele A.; Keefer, Keith D.; Kirchmeier, Robert L.; Shreeve, Jean'ne M.
Journal of the American Chemical Society, 1999 , vol. 121, # 48 p. 11130 - 11138
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydroxide T=40°C; 6 h;
参考文献
Boutevin, B.; Youssef, B.; Boileau, S.; Garnault, A. M.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 399 - 410
反应条件
tetrafluoroboric acid in chloroform-d1
参考文献
Koller, K. L.; Dorn, H. C.
Analytical Chemistry, 1982 , vol. 54, # 3 p. 529 - 533
反应条件
2,2,2-trifluoroethanol; water T=35°C; Kinetics; Reagent/catalyst;
参考文献
Koh, Han Joong; Kang, Suk Jin
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 12 p. 4117 - 4121
反应条件
ethanol; 2,2,2-trifluoroethanol T=35°C; Kinetics; Reagent/catalyst;
参考文献
Koh, Han Joong; Kang, Suk Jin
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 12 p. 4117 - 4121
反应条件
water T=50°C; in var. mixed aqueaus-TFE; Rate constant;
参考文献
Kevill, Dennis N.; Rissmann, Thomas J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , p. 717 - 720
反应条件
T=50°C; various solvents, other substituted allyl arenesulfonates; Rate constant;
参考文献
Kevill, Dennis N.; Rissmann, Thomas J.
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3062 - 3064
反应条件
T=50°C; various solvents, other substituted allyl arenesulfonates; Rate constant;
参考文献
Kevill, Dennis N.; Rissmann, Thomas J.
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3062 - 3064