(2-氨基乙基)-苄基氨基甲酸叔丁酯合成路线 （共 11 条）
反应条件
water; triphenylphosphine in tetrahydrofuran T=0 - 20°C; 23 h;
参考文献
Ji, Haitao; Li, Huiying; Martasek, Pavel; Roman, Linda J.; Poulos, Thomas L.; Silverman, Richard B.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 3 p. 779 - 797
反应条件
hydrazine hydrate in ethanol 24 h; Ambient temperature;
参考文献
Krapcho; Maresch; Lunn
Synthetic Communications, 1993 , vol. 23, # 17 p. 2443 - 2449
反应条件
ammonia; hydrogen; nickel in ethanol
参考文献
Kruijtzer, John A. W.; Lefeber, Dirk J.; Liskamp, Rob M. J.
Tetrahedron Letters, 1997 , vol. 38, # 30 p. 5335 - 5338
反应条件
1: 99 percent / NaOH 2: 87 percent / H2, NH3 / Raney-Ni / ethanol View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 30 p. 5335 - 5338
反应条件
1: 88 percent 2: 99 percent / NaOH 3: 87 percent / H2, NH3 / Raney-Ni / ethanol View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 30 p. 5335 - 5338
反应条件
diborane in tetrahydrofuran Yield given;
参考文献
Tetrahedron Letters, , vol. 38, # 30 p. 5335 - 5338
反应条件
1: Et3N 2: 25percent NH3(H2O) 3: B2H6 / tetrahydrofuran View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 30 p. 5335 - 5338
反应条件
1: sodium carbonate / |Reflux; |Inert atmosphere; |Dean-Stark 2: 0.5 h / 0 - 20 °C / |Inert atmosphere; |Dean-Stark 3: water / isopropyl alcohol / 50 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 9, # 1 p. 102 - 104
反应条件
1: 91 percent / CH2Cl2 / 24 h / Ambient temperature 2: 78 percent / diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / 14 h 3: 90 percent / 55percent aq. hydrazine hydrate / ethanol / 24 h / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 23, # 17 p. 2443 - 2449
反应条件
1: 78 percent / diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / 14 h 2: 90 percent / 55percent aq. hydrazine hydrate / ethanol / 24 h / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 23, # 17 p. 2443 - 2449
