乙基(2-羟基乙基)氨基甲酸叔丁酯合成路线 (共 4 条)
反应条件
in dichloromethane 24 h; Ambient temperature;
参考文献
Krapcho; Maresch; Lunn
Synthetic Communications, 1993 , vol. 23, # 17 p. 2443 - 2449
反应条件
triethylamine in 1,4-dioxane; water
参考文献
Merck and Co., Inc.
Patent: US6316444 B1, 2001 ;
US 6316444 B1
反应条件
1: 81 percent / diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / 14 h 2: 72 percent / 55percent aq. hydrazine hydrate / ethanol / 24 h / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 23, # 17 p. 2443 - 2449
反应条件
1H-imidazole; iodine; triphenylphosphine in dichloromethane
T=20°C;
参考文献
Wendt, Barbara; Ha, Huy Riem; Hesse, Manfred
Helvetica Chimica Acta, 2002 , vol. 85, # 9 p. 2990 - 3001