N-Boc-1H-吡唑-1-甲脒合成路线 （共 5 条）
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 2 h;
参考文献
Schroif-Gregoire, Cosima; Barale, Karine; Zaparucha, Anne; Al-Mourabit, Ali
Tetrahedron Letters, 2007 , vol. 48, # 13 p. 2357 - 2359
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane; N,N-dimethyl-formamide T=20°C; 2 h;
参考文献
Castillo-Melendez, Joel A.; Golding, Bernard T.
Synthesis, 2004 , # 10 p. 1655 - 1663
反应条件
N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide 0.666667 h; Ambient temperature;
参考文献
Wu; Matsueda; Bernatowicz
Synthetic Communications, 1993 , vol. 23, # 21 p. 3055 - 3060
反应条件
1: tert-butyl (1H-pyrazol-1-ylcarbonoimidoyl)carbamate With sodium hydride in tetrahydrofuran T=-5 - 0°C; 1.5 h; 2: di-tert-butyl dicarbonate in tetrahydrofuran T=-5 - 0°C; 2 h; Heating / reflux; Product distribution / selectivity;
参考文献
WO2008/126943 A2, ;
Page/Page column 79-80 ;
反应条件
N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide T=20°C; 2.66667 h; Product distribution / selectivity;
参考文献
WO2008/126943 A2, ;
Page/Page column 78-79 ;
