2,5-二(二甲基氨基)-P-苯醌合成路线 (共 7 条)
反应条件
copper diacetate; oxygen; potassium thioacyanate; potassium thioacyanate; copper diacetate in N,N-dimethyl-formamide T=49 - 102°C; P=25742.8 Torr; 0.5 h; variable reaction time, different concentrations of catalysts, steel and PTFE-lined reactors; Rate constantProduct distribution;
参考文献
Beltrame, Paolo; Beltrame, Pier Luigi; Bussola, Marzio; Carniti, Paolo
Gazzetta Chimica Italiana, 1980 , vol. 110, # 2/3 p. 141 - 146
参考文献
Harger
Journal of the American Chemical Society, 1924 , vol. 46, p. 2547
参考文献
Kehrmann
Chemische Berichte, 1890 , vol. 23, p. 904
反应条件
copper diacetate; potassium thioacyanate; potassium thioacyanate; copper diacetate in N,N-dimethyl-formamide T=70°C; 5.5 h; other object: decomposition in solution; Rate constant;
参考文献
Beltrame, Paolo; Beltrame, Pier Luigi; Bussola, Marzio; Carniti, Paolo
Gazzetta Chimica Italiana, 1980 , vol. 110, # 2/3 p. 141 - 146
参考文献
Kehrmann
Chemische Berichte, 1890 , vol. 23, p. 904
反应条件
in ethanol; isopropyl alcohol T=0°C; 4 h;
参考文献
Ott; Pinter
Monatshefte fur Chemie, 1997 , vol. 128, # 8-9 p. 901 - 909
参考文献
Harger
Proceedings of the National Academy of Sciences of the United States of America, vol. 8, p. 57
Chem. Zentralbl., 1922 , vol. 93, # III p. 355
Full Text Show Details
Harger
Journal of the American Chemical Society, 1924 , vol. 46, p. 2547