1: phenyl-(9-BBN) With lithium tert-butylate in 2-methyl-propan-1-ol; benzene T=20°C; 0.333333 h; Schlenk techniqueInert atmosphere; 2: (3-bromo-3-methyl-n-butyl)benzene With [(diglyme)NiBr2]; 4,4'-di-tert-butyl-2,2'-dipyridyl in 2-methyl-propan-1-ol; benzene T=20 - 40°C; Suzuki Coupling; 28.5 h; Schlenk techniqueInert atmosphere;

sodium isopropanolate; sodium T=125°C;

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1: Al 2: (i) H2, PtO2, AcOH, (ii) Ac2O, (iii) Pd-C View Scheme

1: Al 2: (i) H2, PtO2, AcOH, (ii) Ac2O, (iii) Pd-C View Scheme