(S)-(+)-1-苯基-2-丙醇合成路线 (共 70 条)
反应条件
D-glucopyranose in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=8; 4 h; enantioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 12 p. 3120 - 3124
Angew. Chem., , vol. 126, # 12 p. 3348,1
反应条件
1: L-Selectride / tetrahydrofuran / 1 h / -78 °C 2: 67 percent / tert-butyllithium / tetrahydrofuran / 0.17 h / -78 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 70, # 5 p. 1796 - 1801
反应条件
1.1: n-BuLi / tetrahydrofuran / 0.5 h / -30 °C 1.2: 68 percent / tetrahydrofuran / 1 h / 20 °C 2.1: Sphingomonas paucimobilis NCIMB 8195 / dimethylformamide; H2O; various solvent(s) / 120 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 66, # 19 p. 6495 - 6497
反应条件
1: 73 percent / aq. NaOH / 0.75 h / 65 °C 2: 86 percent / LiAlH4 / diethyl ether / 2 h / Heating View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 9, # 22 p. 4021 - 4026
反应条件
lipase AK from Pseudomonas fluorescens in tetrahydrofuran; hexane T=30°C; 4 h; Sealed tube; optical yield given as percent ee;
参考文献
Process Biochemistry, , vol. 47, # 3 p. 428 - 434
反应条件
D-glucopyranose in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=8; 4 h; enantioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 12 p. 3120 - 3124
Angew. Chem., , vol. 126, # 12 p. 3348,1
反应条件
lipase from Pseudomonas cepacia immobilized on ceramic in toluene T=40°C; 4 h;
参考文献
Monatshefte fur Chemie, , vol. 134, # 8 p. 1151 - 1157
反应条件
Burkholderia cepacia lipase immobilized on ceramic particles in hexane T=20°C; 48 h;
参考文献
Tetrahedron Asymmetry, , vol. 17, # 15 p. 2220 - 2234
反应条件
Burkholderia cepacia lipase immobilized on ceramic particles in hexane T=20°C; 48 h;
参考文献
Tetrahedron Asymmetry, , vol. 17, # 15 p. 2220 - 2234
反应条件
D-glucopyranose in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=8; 4 h; Reagent/catalyst; enantioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 12 p. 3120 - 3124
Angew. Chem., , vol. 126, # 12 p. 3348,1