(E)-1,1,1,2,3,4,4,4-八氟丁-2-烯合成路线 (共 13 条)
反应条件
T=816.9°C; gas-phase reaction in Xe, heating by pulsed adiabatic compression, various maximum temperature in adiabatic compression pulse; Equilibrium constant;
参考文献
Buravtsev, N. N.; Kolbanovskii, Yu. A.; Ovsyannikov, A. A.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 12 p. 1891 - 1900
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 12 p. 1802 - 1809
反应条件
T=816.9°C; gas-phase reaction in Xe, heating by pulsed adiabatic compression, various maximum temperature in adiabatic compression pulse; Equilibrium constant;
参考文献
Buravtsev, N. N.; Kolbanovskii, Yu. A.; Ovsyannikov, A. A.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 12 p. 1891 - 1900
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 12 p. 1802 - 1809
反应条件
dimethyl cadmium in acetonitrile
T=-196 - 20°C; Title compound not separated from byproducts;
参考文献
Nair, Haridasan K.; Burton, Donald J.
Journal of Fluorine Chemistry, 1992 , vol. 56, # 3 p. 341 - 351
反应条件
potassium fluoride; 18-crown-6 ether in sulfolane
T=190°C; 48 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chambers, Richard D.; Edwards, Andrew R.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 24 p. 3623 - 3627
反应条件
in neat (no solvent)
pyrolysis at 180°C, 10-200 Torr;
参考文献
Sharp; Coyle
Inorganic Chemistry, 1972 , vol. 11, p. 1259,1260, 1261
反应条件
byproducts: SiF4; at 420 Torr and 200°C (1 h);
参考文献
Sharp; Schwager
Inorganic Chemistry, 1976 , vol. 15, p. 1697
反应条件
SbF5
T=20°C; 5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chepik, S. D.; Petrov, V. A.; Galakhov, M. V.; Belen'kii, G. G.; Mysov, E. I.; German, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 8.2 p. 1674 - 1680
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 8 p. 1844 - 1851
反应条件
zinc in ethanol
Product distribution;
参考文献
Filyakova, T. I.; Kodess, M. I.; Peschanskii, N. V.; Zapevalov, A. Ya.; Kolenko, I. P.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 9 p. 1651 - 1658
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 9 p. 1858 - 1866
反应条件
cesium fluoride in diethylene glycol dimethyl ether
7 h; Heating; Product distribution;
参考文献
Filyakova, T. I.; Kodess, M. I.; Peschanskii, N. V.; Zapevalov, A. Ya.; Kolenko, I. P.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 9 p. 1651 - 1658
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 9 p. 1858 - 1866
反应条件
dibenzo-18-crown-6
T=180°C; 1 h; other potassium salts of perfluorocarboxylic acids; Product distribution;
参考文献
Podol'skii, A. V.; Khonina, T. G.; Filyakova, T. I.; Kachalkova, M. I.; Kodess, M. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 10 p. 1977 - 1979
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 10 p. 2259 - 2261