potassium fluoride; copper monoiodide in diethyl ether; ethyl acetate; N,N-dimethyl-formamide

1: 1-Amino-2-chloro-4-nitrobenzene With hydrogenchloride in water T=0°C; 0.0833333 h; Inert atmosphereSchlenk technique; 2: With tert.-butylnitrite T=0°C; 0.25 h; Inert atmosphereSchlenk technique; 3: trifluoromethylsilver T=-78 - 20°C; 4 h; Inert atmosphereSchlenk technique;

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potassium fluoride; tetra-phenylphosphonium bromide in dimethyl sulfoxide T=130°C; 5 h;