2-(4-甲基苯氧基)乙醇合成路线 （共 16 条）
反应条件
phosphorus tribromide
参考文献
Marona, Henryk; Antkiewicz-Michaluk, Lucyna
Acta Poloniae Pharmaceutica - Drug Research, 1998 , vol. 55, # 6 p. 487 - 498
反应条件
[bis(acetoxy)iodo]benzene; iodine in 1,2-dichloro-ethane T=60 - 70°C; Irradiation;
参考文献
Muraki; Togo; Yokoyama
Tetrahedron Letters, 1996 , vol. 37, # 14 p. 2441 - 2444
反应条件
1: 76.8 percent / SOCl2 / toluene / 1 h / 90 °C 2: 1.) 60percent NaH / 1.) DMF, 80 deg C, 30 min, 2.) DMF, 100 deg C, 4 h 3: KOH, H2O / ethanol / 3 h / Ambient temperature 4: 19.9 g / piperidine / pyridine / 4 h / 65 °C 5: KOH, H2O / ethanol / 8 h / Ambient temperature 6: 87.3 percent / aq. K2CO3 / dimethylformamide / 2 h / 30 °C View Scheme
参考文献
Kawashima; Kameo; Kato; Hasegawa; Tomisawa; Hatayama; Hirono; Moriguchi
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 3 p. 774 - 777
参考文献
Kuliev,S.N. et al.
Journal of Organic Chemistry USSR (English Translation), 1976 , vol. 12, p. 2451 - 2453
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 12 p. 2533 - 2535
参考文献
Kuliev,S.N. et al.
Journal of Organic Chemistry USSR (English Translation), 1976 , vol. 12, p. 2451 - 2453
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 12 p. 2533 - 2535
反应条件
1: SOCl2; pyridine; CHCl3
2: 120 °C
3: SOCl2; CHCl3
View Scheme
参考文献
Gump; Nikawitz
Journal of the American Chemical Society, 1950 , vol. 72, p. 3846,3848, 3850
