2-氯-2,2-二氟乙酸甲酯合成路线 （共 95 条）
反应条件
potassium fluoride; copper(l) iodide in N,N-dimethyl-formamide T=100°C; 10 h;
参考文献
Su, De-Bao; Duan, Jian-Xing; Chen, Quing-Yun
Tetrahedron Letters, 1991 , vol. 32, # 52 p. 7689 - 7690
反应条件
1: With potassium fluoride; copper(l) iodide in N,N-dimethyl-formamide T=125°C; 13 h; 2: With ammonia; ammonium chloride in water; N,N-dimethyl-formamide T=20°C; 1.5 h;
参考文献
EP2128158 A1, ;
Page/Page column 20-21 ;
EP 2128158 A1
反应条件
methanol; zinc T=50°C; 1 - 4 h; Heating / reflux; Product distribution / selectivity;
参考文献
EP1574496 A1, ;
Page/Page column 2; 3 ;
反应条件
potassium fluoride; copper(l) iodide in N,N-dimethyl acetamide T=120°C; Reagent/catalystTemperatureConcentration;
参考文献
Organic Process Research and Development, , vol. 17, # 6 p. 940 - 945
反应条件
N,N'-dimethyl-N,N'-propyleneurea; potassium fluoride; copper(l) iodide heating;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 2 p. 225 - 228
反应条件
potassium fluoride; copper(l) iodide in N,N-dimethyl-formamide T=100 - 120°C; 8 h; other solvent; other organic halides; Product distributionMechanism;
参考文献
Su, De-Bao; Duan, Jian-Xing; Chen, Quing-Yun
Tetrahedron Letters, 1991 , vol. 32, # 52 p. 7689 - 7690
反应条件
potassium fluoride; copper(l) iodide; iodine in N,N-dimethyl-formamide T=120°C; 3 h;
参考文献
Journal of the Chemical Society - Series Chemical Communications, , # 11 p. 807 - 808
反应条件
copper(l) iodide; iodine; potassium iodide in N,N-dimethyl-formamide T=120°C; 3 h; Yield given;
参考文献
Su; Duan; Chen
Journal of the Chemical Society - Series Chemical Communications, 1992 , # 11 p. 807 - 808
反应条件
potassium fluoride; copper(l) iodide; iodine in N,N-dimethyl-formamide T=120°C; 3 h; other bromodifluoroacetate deriv.; var. temp. and times of reaction; Mechanism;
参考文献
Journal of the Chemical Society - Series Chemical Communications, , # 11 p. 807 - 808
反应条件
potassium fluoride; copper(l) iodide in N,N-dimethyl-formamide T=110 - 120°C; 8 h;
参考文献
Tetrahedron Letters, , vol. 32, # 52 p. 7689 - 7690
