二(2,2,2-三氟乙基)碳酸酯合成路线 (共 4 条)
反应条件
potassium fluoride; zirconium oxide T=140°C; 10 h; pressure tight reactor;
参考文献
Asahi Glass Co., Ltd.
Patent: EP2218708 A1, 2010 ;
Location in patent: Page/Page column 21; 22 ;
反应条件
triethylamine in N,N-dimethyl-formamide; 1,2-dichloro-benzene T=0 - 20°C;
参考文献
Bogolubsky, Andrey V.; Ryabukhin, Sergey V.; Pipko, Sergey E.; Lukin, Oleg; Shivanyuk, Alexander; Mykytenko, Dmytro; Tolmachev, Andrey
Tetrahedron, 2011 , vol. 67, # 20 p. 3619 - 3623
反应条件
pyridine in diethyl ether
参考文献
Krespan, Carl G.; Smart, Bruce E.
Journal of Organic Chemistry, 1986 , vol. 51, # 3 p. 320 - 326
反应条件
sodium methylate in toluene
参考文献
General Electric Company
Patent: US4349486 A1, 1982 ;