beta-雌二醇17-(beta-D-葡糖苷酸)钠盐合成路线 (共 5 条)
反应条件
sodium hydroxide in methanol Ambient temperature;
参考文献
Numazawa, Mitsuteru; Nagaoka, Masao; Tsuji, Masachika; Osawa, Yoshio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 1 p. 121 - 125
反应条件
1: 72 percent / Ag2CO3 / benzene / 48 h / Ambient temperature 2: 83 percent / NaBH4, PdCl2 / methanol / 2 h / 0 °C 3: 44 percent / aq. 2M NaOH / methanol / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 121 - 125
反应条件
1: 83 percent / NaBH4, PdCl2 / methanol / 2 h / 0 °C 2: 44 percent / aq. 2M NaOH / methanol / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 121 - 125
反应条件
1: 72 percent / Ag2CO3 / benzene / 48 h / Ambient temperature 2: 83 percent / NaBH4, PdCl2 / methanol / 2 h / 0 °C 3: 44 percent / aq. 2M NaOH / methanol / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 121 - 125
反应条件
T=38°C; 24 h; beef-liver β-glucuronidase, 0.1M acetate buffer (pH 4.6);
参考文献
Numazawa, Mitsuteru; Nagaoka, Masao; Tsuji, Masachika; Osawa, Yoshio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 1 p. 121 - 125