反应条件
1: 1.) O3, 2.) NaBH4 / 1.) CH2Cl2, CH3OH, -78 deg C, 10 min, 2.) CH2Cl2, CH3OH, -78 deg C, 10 min 2: 77 percent / pyridine, DMAP / CH2Cl2 / 40 °C 3: 81 percent / BuSnH, AlBN / toluene / 90 °C 4: 52 percent / Na, naphthalene / tetrahydrofuran / -78 °C View Scheme
参考文献
Trost, Barry M.; Marrs, Christopher M.
Journal of the American Chemical Society, 1993 , vol. 115, # 15 p. 6636 - 6645