2-甲基-3-苯基-2-丙烯-1-醇合成路线 （共 52 条）
反应条件
sodium tetrahydroborate in ethanol
参考文献
TAKASAGO INTERNATIONAL CORPORATION
Patent: US2011/201819 A1, 2011 ;
Location in patent: Page/Page column 8 ;
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether
参考文献
Falciola, Caroline A.; Tissot-Croset, Karine; Alexakis, Alexandre
Angewandte Chemie - International Edition, 2006 , vol. 45, # 36 p. 5995 - 5998
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 10 h; Inert atmosphere;
参考文献
Jiang, Tao; Huynh, Khoi; Livinghouse, Tom
Synlett, 2013 , vol. 24, # 2 art. no. ST-2012-P0768-SP, p. 193 - 196
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 1 h;
参考文献
Daub, G. William; Edwards, James P.; Okada, Carol R.; Allen, Jana Westran; Maxey, Claudia Tata; Wells, Matthew S.; Goldstein, Alexandra S.; Dibley, Michael J.; Wang, Clarence J.; Ostercamp, Daniel P.; Chung, Steven; Cunningham, Paula Shanklin; Berliner, Martin A.
Journal of Organic Chemistry, 1997 , vol. 62, # 7 p. 1976 - 1985
反应条件
lithium aluminium tetrahydride; ethanol in diethyl ether T=-78 - 20°C; 0.5 h;
参考文献
Ramachandran, P. Veeraraghavan; Burghardt, Thomas E.; Reddy, M. Venkat Ram
Tetrahedron Letters, 2005 , vol. 46, # 12 p. 2121 - 2124
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 1 h;
参考文献
Basavaiah, Deevi; Sarma, Pakala K. S.
Journal of the Chemical Society, Chemical Communications, 1992 , # 13 p. 955 - 957
反应条件
dicobalt octacarbonyl; water in ethylene glycol dimethyl ether 2 h; Heating;
参考文献
Tetrahedron Letters, , vol. 44, # 14 p. 2775 - 2778
反应条件
potassium dihydrogenphosphate; (NH4)HPO4; magnesium sulfate in water T=28 - 32°C; 4 h; commercial baker's yeast, sugar beet molasses; Title compound not separated from byproducts;
参考文献
Fronza, Giovanni; Fuganti, Claudio; Grasselli, Piero; Majori, Luisella; Pedrocchi-Fantoni, Giuseppe; Spreafico, Franca
Journal of Organic Chemistry, 1982 , vol. 47, # 17 p. 3289 - 3296
反应条件
1: 3-phenyl-2-propyn-1-ol (phenyl propargyl alcohol) With lithium hydride in tetrahydrofuran T=0°C; alcoholate formation; 1 h; 2: CH3Li*CeCl3 in tetrahydrofuran T=-78 - -20°C; Addition; 24 h;
参考文献
Bartoli, Giuseppe; Bellucci, M. Cristina; Bosco, Marcella; Dalpozzo, Renato; De Nino, Antonio; Sambri, Letizia; Tagarelli, Antonio
European Journal of Organic Chemistry, 2000 , # 1 p. 99 - 104
反应条件
bis(1,5-cyclooctadiene)nickel (0); water; caesium carbonate; tri-cyclo-hexyl-phosphine in toluene T=75°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Bausch, Cory C.; Patman, Ryan L.; Breit, Bernhard; Krische, Michael J.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 25 p. 5687 - 5690
