1,4-二甲基-1,2-二氢吡啶-2-酮合成路线 （共 10 条）
反应条件
potassium carbonate in methanol
22 h; Reflux;
参考文献
Nakao, Yoshiaki; Idei, Hiroaki; Kanyiva, Kyalo Stephen; Hiyama, Tamejiro
Journal of the American Chemical Society, 2009 , vol. 131, # 44 p. 15996 - 15997
反应条件
methanol; sodium methylate
参考文献
Adams; Schrecker
Journal of the American Chemical Society, 1949 , vol. 71, p. 1186,1191
反应条件
Bei laengerem Erhitzen auf 210grad;
参考文献
Wiberg et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 3160,3164
反应条件
1: 61 percent / potassium carbonate, molecular sieve / diethyl ether
2: 78 percent / 0 h / 350 °C
View Scheme
参考文献
Eberbach, Wolfgang; Roser, Joachim
Tetrahedron Letters, 1987 , vol. 28, # 24 p. 2689 - 2692
反应条件
potassium hydroxide; hydrazine hydrate; ethylene glycol
参考文献
Sugasawa; Kirisawa
Chemical and Pharmaceutical Bulletin, 1958 , vol. 6, p. 615,617
反应条件
1: toluene-4-sulfonic acid; benzene
2: anschliessende Oxidation mit K3<Fe(CN)6>
3: water; hydrochloric acid
4: hydrazine hydrate; potassium hydroxide; ethylene glycol
View Scheme
参考文献
Sugasawa; Kirisawa
Chemical and Pharmaceutical Bulletin, 1958 , vol. 6, p. 615,617
反应条件
1: anschliessende Oxidation mit K3<Fe(CN)6>
2: water; hydrochloric acid
3: hydrazine hydrate; potassium hydroxide; ethylene glycol
View Scheme
参考文献
Sugasawa; Kirisawa
Chemical and Pharmaceutical Bulletin, 1958 , vol. 6, p. 615,617
反应条件
1: water; hydrochloric acid
2: hydrazine hydrate; potassium hydroxide; ethylene glycol
View Scheme
参考文献
Sugasawa; Kirisawa
Chemical and Pharmaceutical Bulletin, 1958 , vol. 6, p. 615,617
参考文献
Wiberg et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 3160,3164
反应条件
nitric acid in acetic anhydride
Ambient temperature;
参考文献
Ariga, Masahiro; Tohda, Yasuo; Matsumura, Eizo
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 1 p. 393 - 394
