1: With sodium methylate in methanol
T=0°C; 0.25 h;
2: With iodine in methanol
T=0 - 20°C;
3: With ammonium hydroxide in methanol
1 h; Heating; Further stages.;
参考文献
Hinze, Claudia; Kreipl, Andreas; Terpin, Andreas; Steglich, Wolfgang
Synthesis, 2007 , # 4 p. 608 - 612
1.1: 76 percent / methanol; diethyl ether / 3 h / 20 °C
2.1: sodium methoxide / methanol / 1 h / 20 °C
2.2: I2 / methanol / 0.5 h / 20 °C
2.3: 37 percent / aq. NH3 / methanol / 1 h / Heating
View Scheme
参考文献
Nishizawa, Tomoyasu; Grueschow, Sabine; Jayamaha, Don-Hema E.; Nishizawa-Harada, Chizuko; Sherman, David H.
Journal of the American Chemical Society, 2006 , vol. 128, # 3 p. 724 - 725
