反应条件
1: 65 percent / tetrahydrofuran / 19 h / Heating 2: 1.) lithium diisopropylamide, oxygen, 2.) dimethylformamide dimethylacetal / 1.) tetrahydrofuran, HMPA, -78 deg C, 30 min, 2.) methylene chloride, -78 deg C -> room temperature 3: 1.) LiAlH4, 2.) TsCl, pyridine, 3.) LiAlH4 View Scheme
参考文献
Paquette, Leo A.; Hertel, Larry W.; Gleiter, Rolf; Boehm, Michael C.; Beno, Mark A.; Christoph, Gary G.
Journal of the American Chemical Society, 1981 , vol. 103, # 24 p. 7106 - 7121
