三（2-甲氧基乙氧基）硼酸合成路线 （共 17 条）
反应条件
boric acid in benzene Substitution; 20 h; Heating;
参考文献
Brzezinski; Gierczyk; Rozalski; Wojciechowski; Schroeder; Zundel
Journal of Molecular Structure, 2000 , vol. 519, # 1-3 p. 119 - 123
反应条件
in 2-methoxy-ethanol boric acid heated with the alcohol for ca. 20 h in Dean-Stark apparatus; solvent evapd. under reduced pressure; borate distd.;
参考文献
Brzezinski; Gierczyk; Rozalski; Wojciechowski; Schroeder; Zundel
Journal of Molecular Structure, 2000 , vol. 519, # 1-3 p. 119 - 123
反应条件
1: With sodium hydrogencarbonate in 2-methoxy-ethanol T=130°C; 21 h; 2: With water 0.5 h; Heating / reflux;
参考文献
Isis Pharmaceuticals Inc.
Patent: US2004/23384 A1, 2004 ;
Location in patent: Page/Page column 19 ;
反应条件
in water converted to the ammonium salt with NH4Cl solution (after removing the biaryls with benzene) and is then reconverted;
参考文献
B: B-Verb.8, 11.2.4.1, page 173 - 175
CZ115040 , ;
C.A., , vol. 64, p. 15922
反应条件
1: With sodium hydrogencarbonate in 2-methoxy-ethanol T=130°C; 21 h; 2: With water 0.5 h; Heating / reflux;
参考文献
Isis Pharmaceuticals Inc.
Patent: US2003/225015 A1, 2003 ;
Location in patent: Page 18-19 ;
反应条件
1: With sodium hydrogencarbonate in 2-methoxy-ethanol T=130°C; 21 h; 2: With water 0.5 h; Heating / reflux;
参考文献
Isis Pharmaceuticals Inc.
Patent: US2003/232770 A1, 2003 ;
Location in patent: Page 18 ;
反应条件
1: With sodium hydrogencarbonate in 2-methoxy-ethanol T=130°C; 21 h; Heating / reflux; 2: With water 0.5 h; Heating / reflux;
参考文献
US2003/224511 A1, ;
Page 18-19 ;
反应条件
1: With sodium hydrogencarbonate in 2-methoxy-ethanol T=130°C; 21 h; 2: With water 0.5 h; Heating / reflux;
参考文献
Isis Pharmaceuticals Inc.
Patent: US2004/23384 A1, 2004 ;
Location in patent: Page/Page column 19 ;
反应条件
1: With sodium hydrogencarbonate in 2-methoxy-ethanol T=130°C; 21 h; 2: With water 0.5 h; Heating / reflux;
参考文献
US2004/5705 A1, ;
Page/Page column 19 ;
反应条件
1: With sodium hydrogencarbonate in 2-methoxy-ethanol T=130°C; 21 h; Heating / reflux; 2: With water 0.5 h; Heating / reflux;
参考文献
Isis Pharmaceuticals Inc.
Patent: US2003/232436 A1, 2003 ;
Location in patent: Page 18 ;
