4-(4-溴苯基)-2,6-二苯基吡啶合成路线 （共 13 条）
反应条件
bismuth trifluoromethanesulphonate; ammonium acetate T=120°C; 2 h; Neat (no solvent);
参考文献
Shinde, Pravin V.; Labade, Vilas B.; Gujar, Jitendra B.; Shingate, Bapurao B.; Shingare, Murlidhar S.
Tetrahedron Letters, 2012 , vol. 53, # 12 p. 1523 - 1527
反应条件
1: With sodium hydroxide 2 h; Inert atmosphere; 2: With ammonium acetate in ethanol 10 h; Inert atmosphereReflux;
参考文献
Jana, Debabrata; Ghorai, Binay K.
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1798 - 1801
反应条件
ammonium acetate in ethanol T=80°C; 10 h;
参考文献
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, , vol. 121, p. 355 - 362
反应条件
sodium hydrogensulfite; copper(I) bromide in dimethyl sulfoxide T=120°C; 2.5 h; Inert atmosphere;
参考文献
Ren, Zhi-Hui; Zhang, Zhi-Yuan; Yang, Bing-Qin; Wang, Yao-Yu; Guan, Zheng-Hui
Organic Letters, 2011 , vol. 13, # 19 p. 5394 - 5397
反应条件
urea; Bi(NO3)3/ZnCl2 on Al2O3 in chloroform T=130°C; 0.3 h; microwave irradiation;
参考文献
Tetrahedron, , vol. 63, # 36 p. 8715 - 8722
反应条件
ammonium acetate; acetic acid 12 h; Reflux;
参考文献
Idemitsu Kosan Co., Ltd.
Patent: US2012/319099 A1, 2012 ;
Location in patent: Page/Page column 41 ;
反应条件
urea; aluminum oxide; Bi(NO3)3 T=130°C;
参考文献
Kumar, Anil; Koul, Summon; Razdan, Tej K.; Kapoor, Kamal K.
Tetrahedron Letters, 2006 , vol. 47, # 5 p. 837 - 842
反应条件
ammonium acetate in acetic acid 12 h; Heating / reflux;
参考文献
IDEMITSU KOSAN CO., LTD.
Patent: WO2006/67931 A1, 2006 ;
Location in patent: Page/Page column 57-58 ;
反应条件
1: With [Hmim][NO3]; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=96°C; Ionic liquidMicrowave irradiation; 2: With ammonium acetate T=96°C; 0.116667 h; Ionic liquidMicrowave irradiation;
参考文献
Khosropour, Ahmad R.; Mohammadpoor-Baltork, Iraj; Kiani, Forough
Comptes Rendus Chimie, 2011 , vol. 14, # 5 p. 441 - 445
反应条件
1: 4-bromobenzyl-alcohol With [Hmim][NO3]; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=96°C; 0.0555556 h; Ionic liquidMicrowave irradiation; 2: acetophenone With ammonium acetate T=96°C; 0.116667 h; Ionic liquidMicrowave irradiation;
参考文献
Khosropour, Ahmad R.; Mohammadpoor-Baltork, Iraj; Kiani, Forough
Comptes Rendus Chimie, 2011 , vol. 14, # 5 p. 441 - 445
