sodium tetrahydroborate; trifluoroacetic acid in dichloromethane T=0°C; 0.166667 h;
参考文献
Ogata, Fujimaro; Takagi, Masato; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the American Chemical Society, 1981 , vol. 103, # 5 p. 1145 - 1153
sodium tetrahydroborate; trifluoroacetic acid in dichloromethane T=0°C; 0.166667 h;
参考文献
Ogata, Fujimaro; Takagi, Masato; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the American Chemical Society, 1981 , vol. 103, # 5 p. 1145 - 1153
sodium tetrahydroborate in diethylene glycol dimethyl ether; water T=20°C; 0.5 h;
参考文献
Ogata, Fujimaro; Takagi, Masato; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the American Chemical Society, 1981 , vol. 103, # 5 p. 1145 - 1153
sodium tetrahydroborate in diethylene glycol dimethyl ether; water T=20°C; 0.5 h; Yield given. Yields of byproduct given;
参考文献
Ogata, Fujimaro; Takagi, Masato; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the American Chemical Society, 1981 , vol. 103, # 5 p. 1145 - 1153
potassium tert-butylate in tert-butyl alcohol 4 h; Heating; Yield given;
参考文献
Ogata, Fujimaro; Takagi, Masato; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the American Chemical Society, 1981 , vol. 103, # 5 p. 1145 - 1153
1: sodium borohydride / bis-(2-methoxy-ethyl) ether; H2O / 0.5 h / 20 °C 2: potassium tert-butoxide / 2-methyl-propan-2-ol / 4 h / Heating View Scheme
参考文献
Ogata, Fujimaro; Takagi, Masato; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the American Chemical Society, 1981 , vol. 103, # 5 p. 1145 - 1153