antimony pentachloride in neat (no solvent) isolation by fractional distillation;;
参考文献
Booth, H. S.; Swinehart, C. F.
Journal of the American Chemical Society, 1935 , vol. 57, p. 1333 - 1342
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Gmelin Handbook: Si: MVol.B, 262, page 708 - 710
Schumb, W. C.; Anderson, H. H.
Journal of the American Chemical Society, 1937 , vol. 59, p. 651 - 653
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Gmelin Handbook: Si: MVol.B, 272, page 732 - 735
in neat (no solvent) byproducts: Br2; on slight warming;;
参考文献
Schumb, W. C.; Anderson, H. H.
Journal of the American Chemical Society, 1937 , vol. 59, p. 651 - 653
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Gmelin Handbook: Si: MVol.B, 272, page 732 - 735
in neat (no solvent) reaction with detonation by strong heating of the mixt. for a short time;; isolation by fractional distillation;;
参考文献
Schumb, W. C.; Gamble, E. L.
Journal of the American Chemical Society, 1932 , vol. 54, p. 3943 - 3949
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Gmelin Handbook: Si: MVol.B, 262, page 708 - 710
in gas passing a SiCl4 containing SiF4 vapor stream through a glass tube, heated up to 600 °C;; condensation at -30 °C and separation by fractionation;;
Fe-Si-alloy in neat (no solvent) reaction with Si-Fe-alloy at 500°C;;
参考文献
Barthes, D.; Chaigneau, M.; Malangeau, P.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1968 , vol. 266, p. 1780 - 1783
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Gmelin Handbook: C: MVol.D2, 4.3.2.5.7, page 372 - 373
