1: 67 percent / Irradiation
2: 1) OH(-), 2) Pb(OCOCH3)4
3: LiAlH4 / diethyl ether / Ambient temperature
5: neat (no solvent) / 0.17 h / 250 °C / In the presence of Ag(1+) lower temperature
View Scheme
1: 67 percent / Irradiation
2: 1) OH(-), 2) Pb(OCOCH3)4
3: ratio of products at 270-310 deg C, 3-10 min, with or without Ag(1+) ions, in solvent or neat.
View Scheme