(Z)-7-十二碳烯-1-醇乙酸酯合成路线 （共 65 条）
反应条件
in dichloromethane 36 h; Further byproducts given;
参考文献
Helvetica Chimica Acta, , vol. 81, # 9 p. 1616 - 1621
反应条件
pyridine in hexane
Acetylation; 2 h;
参考文献
Bykov; Butenko; Egupova; Finkelshtein
Russian Chemical Bulletin, 2000 , vol. 49, # 7 p. 1301 - 1304
反应条件
pyridine in diethyl ether
参考文献
Rossi, Renzo; Carpita, Adriano; Gaudenzi, Loretta; Quirici, Maria Grazia
Gazzetta Chimica Italiana, 1980 , vol. 110, # 4 p. 237 - 246
反应条件
triphenylphosphine hydroiodide; triphenylphospine diiodide in hexane; benzene
1.) 24 h, 0 deg C, 2.) 24 h, room temp.;
参考文献
Sonnet, Philip E.
Synthesis, 1980 , # 10 p. 828 - 830
反应条件
acetic acid
T=60°C; 6 h;
参考文献
Chan, T. H.; Koumaglo, K.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 109 - 120
反应条件
hydrogen; Lindlar's catalyst in hexane
参考文献
Kovalev,B.G.; Ishchenko,R.I.
Journal of Organic Chemistry USSR (English Translation), 1974 , vol. 10, p. 468 - 470
Zhurnal Organicheskoi Khimii, 1974 , vol. 10, # 3 p. 463 - 466
反应条件
1.1: 68.4 percent / MoCl5/SiO2; SnMe4 / toluene / 24 h / 20 °C / 19000 Torr
2.1: 90 percent / LiAlH4; Cp2ZrCl2 / tetrahydrofuran / 2 h
3.1: 9-BBN
3.2: t-BuOK
4.1: LiAlH4
5.1: Py
View Scheme
参考文献
Bykov, Victor I.; Butenko, Tamara A.; Petrova, Elena B.; Finkelshtein, Eugene Sh.
Tetrahedron, 1999 , vol. 55, # 27 p. 8249 - 8252
反应条件
1: 88 percent / KO-tBu, n-BuLi / hexane; diethyl ether / -78 deg C up to RT for 36 h
2: 1.) ICl; 2.) aq. KF / 1.) CCl4, 15 min; 2.) DMSO, RT, 4 h
3: 82 percent / (Ph3P)4Pd / tetrahydrofuran / Ambient temperature
4: 82 percent / HOAc / 6 h / 60 °C
View Scheme
参考文献
Chan, T. H.; Koumaglo, K.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 109 - 120
反应条件
1: 82 percent / (Ph3P)4Pd / tetrahydrofuran / Ambient temperature
2: 82 percent / HOAc / 6 h / 60 °C
View Scheme
参考文献
Chan, T. H.; Koumaglo, K.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 109 - 120
反应条件
1: 95 percent / H2, quinoline / Lindlar catalyst / pentane / 1 h / -10 °C
2: 95 percent / pyridine / diethyl ether
View Scheme
参考文献
Rossi, Renzo; Carpita, Adriano; Gaudenzi, Loretta; Quirici, Maria Grazia
Gazzetta Chimica Italiana, 1980 , vol. 110, # 4 p. 237 - 246
