3-甲基-3,4-二氢-2H-萘-1-酮合成路线 （共 34 条）
反应条件
1: 10.10 g / Raney-Ni / aq. ethanol / 2 h / Heating 2: 79 percent / 75percent H2SO4 / 8 h / 100 °C View Scheme
参考文献
Katsuura, K.; Snieckus, V.
Tetrahedron Letters, 1985 , vol. 26, # 1 p. 9 - 12
反应条件
1: 1.) acetic acid, cc. H2SO4; 2.) acetic acid, cc. H2SO4 / H2O / 1.) 20 h, reflux; 2.) 6 h, reflux 2: 95 percent / polyphosphoric acid / 1.) 95-100 deg C; 2.) 105-115 deg C, 2 h; 3.) rt, 8 h View Scheme
参考文献
Verbel, Joel; Carrie, Robert
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 3-4 p. 116 - 124
反应条件
1: pyridine / Ambient temperature 2: 2-methoxy-ethanol / 2.5 h / Heating 3: 83 percent / conc. H2SO4 / ethanol; H2O / 18 h / Heating 4: 79 percent / 75percent H2SO4 / 8 h / 100 °C View Scheme
参考文献
Katsuura, K.; Snieckus, V.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 124 - 130
反应条件
1: 2-methoxy-ethanol / 2.5 h / Heating 2: 83 percent / conc. H2SO4 / ethanol; H2O / 18 h / Heating 3: 79 percent / 75percent H2SO4 / 8 h / 100 °C View Scheme
参考文献
Katsuura, K.; Snieckus, V.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 124 - 130
反应条件
1: Zn, aq. HCl / toluene / Heating 2: H2SO4 View Scheme
参考文献
Cocker,W. et al.
Journal of the Chemical Society, 1960 , p. 2230 - 2242
反应条件
1: 160 °C 2: Zn, aq. HCl / toluene / Heating 3: H2SO4 View Scheme
参考文献
Cocker,W. et al.
Journal of the Chemical Society, 1960 , p. 2230 - 2242
反应条件
1: (i) Na, (ii) KOH, MeOH 2: 160 °C 3: Zn, aq. HCl / toluene / Heating 4: H2SO4 View Scheme
参考文献
Cocker,W. et al.
Journal of the Chemical Society, 1960 , p. 2230 - 2242
反应条件
1.1: iodine; magnesium / tetrahydrofuran / 2 h / Inert atmosphere; Reflux 1.2: 0 - 20 °C 1.3: 2 h / Reflux 2.1: [(η2-cyclooctene)4Rh2(μ-Cl)2]; 3-methyl-5-(pyrrolidin-1-yl)pyridin-2-amine; aniline; triphenylphosphine; benzoic acid / 2,3,4-trifluorotoluene / 36 h / 100 °C / Inert atmosphere 2.2: 0.17 h View Scheme
参考文献
Beletskiy, Evgeny V.; Sudheer; Douglas, Christopher J.
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5884 - 5893
反应条件
chromium(VI) oxide; acetic acid
参考文献
Burnham,J.W. et al.
Journal of Organic Chemistry, 1974 , vol. 39, # 10 p. 1416 - 1420
反应条件
acetic acid; zinc Behandeln des Reaktionsprodukts mit CrO3 in wss. H2SO4 und Aeton;
参考文献
Julia et al.
Bulletin de la Societe Chimique de France, 1959 , p. 1449,1452
