3-氯-1,1,1,3-四氟丙烷合成路线 (共 36 条)
反应条件
hydrogen fluoride; chlorine; SbCl5 on Shiro Sagi G2X carbon activated by HF, Cl2 at 100 C T=70°C; P=2327.23 Torr; 0.00319444 h; Gas phase; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US7829748 B1, 2010 ;
Location in patent: Page/Page column 5-6 ;
反应条件
SbCl5 on Carbon; hydrogen fluoride T=85°C; 0.000555556 - 0.00277778 h;
参考文献
HONEYWELL INTERNATIONAL INC.; Nair, Haridasan K.; Singh, Rajiv Ratna; Poss, Andrew Joseph; Nalewajek, David
Patent: US2013/211156 A1, 2013 ;
Location in patent: Paragraph 0026 ;
反应条件
hydrogen fluoride; Catalyst M-Chromium oxide P=1018.63 - 5931.67 Torr; 0.00194444 - 0.0111111 h; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2005/245773 A1, 2005 ;
Location in patent: Page/Page column 2; 4 ;
反应条件
hydrogen fluoride; TiClxFy T=30 - 70°C; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2006/58560 A1, 2006 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogen fluoride in sulfolane T=100°C; P=14480.5 Torr; 3 h;
参考文献
Atofina Chemicals, Inc.
Patent: US6362382 B1, 2002 ;
Location in patent: Page column 2 ;
反应条件
hydrogen fluoride; antimony(V) pentachloride T=65 - 70°C; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2006/58560 A1, 2006 ;
Location in patent: Page/Page column 3 ;
反应条件
tetrakis(triphenylphosphine) palladium(0) T=200°C; 48 h; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2005/245773 A1, 2005 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogen fluoride; titanium tetrachloride Product distribution / selectivity;
参考文献
HONEYWELL INTERNATIONAL INC.
Patent: US2012/172636 A1, 2012 ;
Location in patent: Page/Page column 5 ;
反应条件
hydrogen fluoride; chlorine; antimony(V) pentachloride T=90 - 95°C; P=6965.99 Torr;
参考文献
Merkel, Daniel C.; Wang, Haiyou; Pokrovski, Konstantin A.; Tung, Hsueh Sung; Shankland, Ian
Patent: US2012/184786 A1, 2012 ;
Location in patent: Page/Page column 8 ;
反应条件
hydrogen fluoride; antimony(V) pentachloride T=90 - 95°C; P=6965.99 Torr; 500 h;
参考文献
Merkel, Daniel C.; Pokrovski, Konstantin A.; Tung, Hsueh Sung
Patent: US2013/261354 A1, 2013 ;
Location in patent: Paragraph 0106; 0107 ;