1: 53 percent / LiAlH4 / diethyl ether / 1) rt, 24 h, 2) reflux, 1.5 h 2: 65 percent / pyridine / 3 h / 0 °C View Scheme
参考文献
Toeroek, Bela; Molnar, Arpad
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 7 p. 801 - 804
in tetrahydrofuran; diethyl ether; hexane; pentane a) -110 deg C, 2 h, b) to r.t.;
参考文献
Seyferth, Dietmar; Weinstein, Robert M.; Hui, Richard C.; Wang, Wei-Liang; Archer, Colin M.
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5768 - 5773