2,3-二氯-5,8-二羟基-1,4-萘醌合成路线 （共 17 条）
反应条件
1: With AlCl3, aluminium chloride; sodium chloride in neat (no solvent) T=180°C; Friedel-Crafts Acylation; 0.0333333 h; 2: With hydrogenchloride; water Friedel-Crafts Acylation;
参考文献
Guerrero-Vasquez, Guillermo A.; Andrade, Carlos Kleber Z.; Molinillo, Jose M. G.; MacIas, Francisco A.
European Journal of Organic Chemistry, 2013 , # 27 p. 6175 - 6180
反应条件
9,10-dimethoxyanthracene in chloroform 3 h; Ambient temperature;
参考文献
Hayakawa, Kenji; Aso, Mariko; Kanematsu, Ken
Journal of Organic Chemistry, 1985 , vol. 50, # 12 p. 2036 - 2040
反应条件
aluminium trichloride; sodium chloride T=170°C; 0.166667 h;
参考文献
Bekaert, Alain; Andrieux, Jean; Plat, Michel
Bulletin de la Societe Chimique de France, 1986 , # 2 p. 314 - 316
反应条件
Ambient temperature;
参考文献
Hayakawa, Kenji; Aso, Mariko; Kanematsu, Ken
Journal of Organic Chemistry, 1985 , vol. 50, # 12 p. 2036 - 2040
反应条件
aluminium trichloride; sodium chloride T=180°C;
参考文献
Chemische Berichte, , vol. 83, p. 178,180
Journal of the Chemical Society, , p. 1089,1093
反应条件
aluminium trichloride; sodium chloride T=180°C;
参考文献
Chemische Berichte, , vol. 83, p. 178,180
反应条件
1: With iron in acetic acid Dehalogenation; reduction; 0.833333 h; Heating; 2: With oxygen in sodium hydroxide Oxidation; pH=8 - 9;
参考文献
Anufriev, Victor Ph.; Malinovskaya, Galina V.; Novikov, Vyacheslav L.; Balanyova, Nadezhda N.; Polonik, Sergey G.
Synthetic Communications, 1998 , vol. 28, # 12 p. 2149 - 2157
反应条件
sodium carbonate in dimethyl sulfoxide 3 h; Ambient temperature;
参考文献
Chang, He-Xi; Chou, Ting-Chao; Savaraj, Niramol; Liu, Leroy F.; Yu, Chiang; Cheng
Journal of Medicinal Chemistry, 1999 , vol. 42, # 3 p. 405 - 408
反应条件
1.1: tin(ll) chloride; hydrogenchloride / water / 5 h / 140 °C 2.1: potassium hydride / N,N-dimethyl-formamide / -35 - 40 °C / |Inert atmosphere 2.2: |Inert atmosphere View Scheme
参考文献
Guerrero-Vasquez, Guillermo A.; Andrade, Carlos Kleber Z.; Molinillo, Jose M. G.; MacIas, Francisco A.
European Journal of Organic Chemistry, 2013 , # 27 p. 6175 - 6180
反应条件
bromine in acetic acid 10 h; Heating;
参考文献
Horowska; Mazerska; Ledochowski; Cristalli; Franchetti; Martelli
European Journal of Medicinal Chemistry, 1988 , vol. 23, # 1 p. 91 - 96
