1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-十六氟酞菁铜(II) 合成路线 （共 5 条）
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反应条件
14916-87-1 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-十六氟酞菁铜(II)
反应条件
in further solvent(s) 48 h refluxing in α-chloronaphthalene;
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
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反应条件
14916-87-1 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-十六氟酞菁铜(II)
反应条件
CuNaY-zeolite in neat (no solvent) heating of Cu-zeolite (350°C, sealed tube, vac., 2 h), cooling, addn. of tetrafluorophthalonitrile, powdering, evacuation (2 h), heating (300°C, sealed tube, vac., 24 h); extn. (acetone, pyridine, MeCN, acetone; 72 h), drying (90°C, <1 Torr, 15 h); intact complex encapsulated in zeolite;
参考文献
Inorganic Chemistry, , vol. 33, p. 67 - 72
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反应条件
14916-87-1 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-十六氟酞菁铜(II)
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
→
反应条件
14916-87-1 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-十六氟酞菁铜(II)
反应条件
in further solvent(s) N2-atmosphere, 25percent stoich. excess of tetrafluorophthalonitrile, refluxing in 1-chloronaphtalene (24 h); cooling to room temp., filtration, addn. of petroleum ether, cooling in ice bath (pptn.), filtration, recrystn. (H2SO4);
参考文献
Inorganic Chemistry, , vol. 33, p. 67 - 72
→
反应条件
14916-87-1 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-十六氟酞菁铜(II)
反应条件
1: dimethyl sulfoxide View Scheme
参考文献
F: PerFHalOrg.9, 7, page 50 - 101
