in water KAuCl4*2H2O in H2O treated dropwise with stoich. amount of nitrogen donor base in H2O under stirring, pptd.; ppt. filtered off, washed (H2O) 3 times, dried (vac.), elem. anal.;
参考文献
Pitteri, Bruno; Bortoluzzi, Marco
European Journal of Inorganic Chemistry, 2007 , # 28 p. 4456 - 4461
C5H5N in dichloromethane under N2; filtered, dried in vac.; elem. anal.;
参考文献
Hiller, Wolfgang; Belli Dell'Amico, Daniela
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1987 , p. 1329 - 1332
in dichloromethane yield: Ci-{Au(CH2P(S)Ph2)Cl}2 : Cs-{Au2(CH2P(S)Ph2)Cl2} = 20:1;
参考文献
Murray, H. H.; Garzon, Guillermo; Raptis, Raphael G.; Mazany, Anthony M; Porter, Leigh C.; Fackler, John P. Jr.
Inorganic Chemistry, 1988 , vol. 27, p. 836 - 842
