苯基(1-甲基丙基)硫醚合成路线 (共 33 条)
反应条件
1.) THF, hexane, -78 deg C, 0.5 h, 2.) -50 deg C, 5 h, 3.) methyl iodide, 0.5 h, -23 deg C, water; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Cohen, Theodore; Yu, Lin-Chen
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 605 - 608
反应条件
1.) THF, hexane, -78 deg C, 0.5 h, 2.) 0 deg C, 5 h, 3.) methyl iodide, 0.5 h, -23 deg C, water; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Cohen, Theodore; Yu, Lin-Chen
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 605 - 608
反应条件
in methanol
T=20 - 25°C; Substitution; alkylthiodediazoniation; dimerization; Product distribution; Further Variations:reaction times;
参考文献
Barbero, Margherita; Degani, Iacopo; Diulgheroff, Nicola; Dughera, Stefano; Fochi, Rita; Migliaccio, Mara
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5600 - 5608