苯基(1-甲基丙基)硫醚合成路线 （共 33 条）
反应条件
palladium diacetate; CyPF-t-Bu; sodium t-butanolate in ethylene glycol dimethyl ether
T=110°C;
参考文献
Fernandez-Rodriguez, Manuel A.; Shen, Qilong; Hartwig, John F.
Chemistry - A European Journal, 2006 , vol. 12, # 30 p. 7782 - 7796
反应条件
sodium tetrahydroborate; iodine in tetrahydrofuran
T=20°C; 0.166667 h;
参考文献
Karimi, Babak; Zareyee, Daryoush
Synthesis, 2003 , # 3 p. 335 - 336
反应条件
potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in N,N-dimethyl-formamide
T=50°C; 5 h;
参考文献
Ishiyama, Tatsuo; Mori, Masashi; Suzuki, Akira; Miyaura, Norio
Journal of Organometallic Chemistry, 1996 , vol. 525, # 1-2 p. 225 - 231
反应条件
1: thiophenol With sodium hydride in N,N-dimethyl-formamide; mineral oil
T=20 - 70°C; 0.5 h; Inert atmosphere;
2: sec-butyl bromide in N,N-dimethyl-formamide; mineral oil
T=80°C; 1 h; Inert atmosphere;
参考文献
Scholz, Roland; Hellmann, Gunther; Rohs, Susanne; Raabe, Gerhard; Runsink, Jan; Oezdemir, Diana; Luche, Olaf; Hess, Thomas; Giesen, Alexander W.; Atodiresei, Juliana; Lindner, Hans J.; Gais, Hans-Joachim
European Journal of Organic Chemistry, 2010 , # 24 p. 4559 - 4587
反应条件
in tetrahydrofuran; cyclohexane
T=-45°C; 1 h;
参考文献
Cohen,T.; Ritter,R.H.; Oulette,D.
Journal of the American Chemical Society, 1982 , vol. 104, p. 7142
反应条件
CyPF-tBu; palladium diacetate; sodium t-butanolate in ethylene glycol dimethyl ether
T=50°C; Inert atmosphere;
参考文献
Fernandez-Rodriguez, Manuel A.; Hartwig, John F.
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1664 - 1672
反应条件
CyPF-tBu; palladium diacetate; sodium t-butanolate in ethylene glycol dimethyl ether
T=70°C; 4 h; Inert atmosphere;
参考文献
Fernandez-Rodriguez, Manuel A.; Hartwig, John F.
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1664 - 1672
反应条件
1: methyllithium; phenyl vinyl thioether With N,N,N',N,-tetramethylethylenediamine in diethyl ether; hexane
T=0°C; Addition; 2 h;
2: methyl iodide in diethyl ether; hexane
T=0 - 20°C; Methylation; 2 h;
参考文献
Cabiddu, Maria Grazia; Cabiddu, Salvatore; Cadoni, Enzo; Cannas, Rita; Fattuoni, Claudia; Melis, Stefana
Tetrahedron, 1998 , vol. 54, # 46 p. 14095 - 14104
反应条件
sec.-butyllithium in diethyl ether
T=-78 - 0°C; 1.) -78 deg C, 0.5 h, 2.) -50 deg C, 2.5 h, 3.) 0 deg C, 5 h;
参考文献
Cohen, Theodore; Yu, Lin-Chen
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 605 - 608
反应条件
in methanol
T=18°C; 0.3 h; Irradiation;
参考文献
Deniau, Jean; Duong, Kiem N. V.; Gaudemer, Alain; Bougeard, Peter; Johnson, Michael D.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 393 - 398
