二氯二[1,1'-硫代二[乙烷]]铂合成路线 （共 23 条）
反应条件
in benzene To a benzene soln. of complex was added a soln. of slightly excess LiBr or MesLi in ether;; not sepd., detected by UV-spectroscopy;;
参考文献
Tobita, Hiromi; Habazaki, Hiroki; Ogino, Hiroshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 797 - 799
反应条件
in benzene-d6 byproducts: SEt2; (N2); using Schlenk techniques; mixing of PtCl2(SEt2)2 and Au(C6H3(CH2NMe2)2)(PPh3) in 1:1 molar ratio in C6D6; reflux for 2 h; detected by NMR;
参考文献
Contel, Maria; Stol, Marianne; Casado, Miguel A.; Van Klink, Gerard P.M.; Ellis, Dianne D.; Spek, Anthony L.; Van Koten, Gerard
Organometallics, 2002 , vol. 21, # 21 p. 4556 - 4559
反应条件
N(C2H5)3 in methanol stirred for 16 h; filtered, filtrate evapd., dissolved in CH2Cl2, dried in vac., crystn. (CH2Cl2-diethyl ether); elem. anal.;
参考文献
Yamazaki, Shinsaku; Ama, Tomoharu; Taira, Zenei
Polyhedron, 1988 , vol. 7, p. 353 - 362
反应条件
in neat (no solvent) refluxing in excess of COD for 2 h (crystn.); collection (filtration), washing (hexane), drying (vac.); elem. anal.;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 289 - 292
反应条件
in water Irradiation (UV/VIS); dissolving in H2O on shaking for 48 h; pptn. on irradiation with a quartz-mercury-lamp;; recrystallization in ether;;
参考文献
Cross, Ronald J.; Green, Thomas H.; Keat, Rodney
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 382 - 384
反应条件
in benzene To a benzene soln. of complex was added a soln. of slightly excess LiBr or MesLi in ether;; not sepd., detected by UV-spectroscopy;;
参考文献
Tobita, Hiromi; Habazaki, Hiroki; Ogino, Hiroshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 797 - 799
反应条件
in water Irradiation (UV/VIS); dissolving in H2O on shaking for 48 h; pptn. on irradiation with a quartz-mercury-lamp;; recrystallization in ether;;
参考文献
Cross, Ronald J.; Green, Thomas H.; Keat, Rodney
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 382 - 384
反应条件
in benzene To a benzene soln. of complex was added a soln. of slightly excess LiBr or MesLi in ether;; not sepd., detected by UV-spectroscopy;;
参考文献
Tobita, Hiromi; Habazaki, Hiroki; Ogino, Hiroshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 797 - 799
反应条件
in water Irradiation (UV/VIS); dissolving in H2O on shaking for 48 h; pptn. on irradiation with a quartz-mercury-lamp;; recrystallization in ether;;
参考文献
Cross, Ronald J.; Green, Thomas H.; Keat, Rodney
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 382 - 384
反应条件
in benzene To a benzene soln. of complex was added a soln. of slightly excess LiBr or MesLi in ether;; not sepd., detected by UV-spectroscopy;;
参考文献
Tobita, Hiromi; Habazaki, Hiroki; Ogino, Hiroshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 797 - 799
