二氯二[1,1'-硫代二[乙烷]]铂合成路线 （共 23 条）
反应条件
in water byproducts: KCl; (inert atm.); addn. of diethylsulfide to aq. soln. of platinum compd., stirring for 24 h; evapn. at 25°C in vac., extn. (hot benzene), filtration, concg., cooling to 0°C, filtration, washing with hexane, NMR;
参考文献
De Crisci, Antonio G.; Lough, Alan J.; Multani, Kanwarpal; Fekl, Ulrich
Organometallics, 2008 , vol. 27, # 8 p. 1765 - 1779
反应条件
in water Irradiation (UV/VIS); dissolving in H2O on shaking for 48 h; pptn. on irradiation with a quartz-mercury-lamp;; recrystallization in ether;;
参考文献
Cross, Ronald J.; Green, Thomas H.; Keat, Rodney
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 382 - 384
反应条件
in water shaking of a soln. of K2(PtCl4) in H2O with S(C2H5)2; sucking off;; washing with H2O; recrystallization in alcohol for 1 time and 2-3 times in ether;;
参考文献
Blomstrand, C. W.
Journal fuer Praktische Chemie (Leipzig), 1888 , vol. 38, p. 345 - 365
Full Text Show Details
Gmelin Handbook: Pt: MVol.D, 137, page 307 - 309
反应条件
in water heating of aq. H2(PtCl6)-soln. with S(C2H5)2 in a closed tube;; extraction with boiling alcohol;;
参考文献
Jensen, K. A.
Z. Anorg. Chem., 1935 , vol. 225, p. 115 - 141
Full Text Show Details
Gmelin Handbook: Pt: MVol.D, 208, page 459 - 461
反应条件
in water heating of aq. PtCl4-soln. with S(C2H5)2 in a closed tube;; extraction with boiling alcohol;;
参考文献
Gmelin Handbook: Pt: MVol.D, 137, page 307 - 309
反应条件
1: hydrogenchloride 2: water View Scheme
参考文献
Gmelin Handbook: Pt: MVol.D, 138, page 309 - 311
反应条件
1: hydrogenchloride 2: water View Scheme
参考文献
Gmelin Handbook: Pt: MVol.D, 138, page 309 - 311
反应条件
in methanol; water Kinetics; byproducts: Cl(1-); 95percent MeOH, 5percent H2O; 25.0°C;; elem. anal.;
参考文献
Tobe, Martin L.; Treadgold, Andrew T.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 2347 - 2352
反应条件
in water shaking with diethyl sulfide in water;;
参考文献
Gmelin Handbook: Pt: MVol.D, 135, page 302 - 304
反应条件
1: not given 2: water View Scheme
参考文献
Gmelin Handbook: Pt: MVol.D, 91, page 216 - 219
