双(氰苯)二氯铂(II)合成路线 (共 24 条)
反应条件
in benzene according to R. Bender, P. Braunstein, A. Tiripicchio and C. M. Tiripicchio, J. Chem. Soc., Chem. Commun., 42 (1984); CO atm.; mixture stirred (4 h); homogenization step; after 15 min yellow ppt.;; washing (benzene/hexane); dried in vac.;;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, p. 2360 - 2362,2188 - 2190
参考文献
Zarate, Eugene A.; Tessier-Youngs, Claire A.; Youngs, Wiley J.
Journal of the American Chemical Society, 1988 , vol. 110, p. 4068 - 4070
反应条件
PPh3 in not given
inert atmosphere; mixing at -76°C, warming to 25°C; chromy.;
参考文献
Bender, Robert; Braunstein, Pierre; Richert, Jean-Luc; Dusausoy, Yves
New Journal of Chemistry, 1990 , vol. 14, p. 569 - 582
反应条件
in chloroform-d1
byproducts: ethane; in NMR tube; 60°C for a few h; filtered; evapn. to dryness; detn. by NMR and MS;
参考文献
Molter, Anja; Mohr, Fabian
Zeitschrift fur Anorganische und Allgemeine Chemie, 2009 , vol. 635, # 1 p. 134 - 138