反应条件
1: 96 percent / LiAlH4 / tetrahydrofuran; diethyl ether / 4 h / Heating
2: 90 percent / NaOH / CTAB / CH2Cl2 / 12 h / 25 °C
3: 76 percent / acetonitrile / 0.5 h / 0 °C
4: 71 percent / BBr3 / CH2Cl2 / 12 h / 0 - 25 °C
5: 86 percent / CAN / acetonitrile / 0.17 h / 0 °C
6: 36 percent / dithienyl ditelluride, NaBH4, NaOH / tetrahydrofuran; H2O / 6 h / 67 °C
7: 76 percent / 10percent NaOH / methanol / 0.5 h / 25 °C
View Scheme
参考文献
Sadanandan, E. V.; Cava, Michael P.
Tetrahedron Letters, 1993 , vol. 34, # 15 p. 2405 - 2408
