hydrogen; (o-OC6H4CH3)3PRuCl(PPh3)2 in benzene
the reaction was carried out in two steps (beetwen them the reaction mixture was exposed to air); 1.) p=65 psi, 120 deg C, 2 h, 2.) p=70 psi, 95 deg C, 17 h; Product distribution;
参考文献
Lewis,L.N.
Journal of the American Chemical Society, 1986 , vol. 108, p. 743
5,6,8,9-tetrahydro-7-phenyldibenzolt;c,hgt;xanthenylium tetrafluoroborate in dichloromethane
T=20°C; 120 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Katritzky, Alan R.; Lloyd, Jeremy M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 10 p. 2347 - 2352
