1,1'-(1-环戊烯-1,2-二基)二苯合成路线 （共 20 条）
反应条件
potassium permanganate; sodium periodate; potassium carbonate
参考文献
Curtin,D.Y. et al.
Journal of Organic Chemistry, 1971 , vol. 36, # 4 p. 565 - 572
反应条件
formic acid T=100°C; Equilibrium constantThermodynamic data;
参考文献
Rio,G.; Bricout,D.
Bulletin de la Societe Chimique de France, 1971 , p. 3557 - 3560
反应条件
formic acid
8 h; Heating;
参考文献
Somers, J. B. M.; Couture, A.; Lablache-Combier, A.; Laarhoven, W. H.
Journal of the American Chemical Society, 1985 , vol. 107, # 5 p. 1387 - 1394
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran
Heating;
参考文献
Baumstark,A.L. et al.
Journal of Organic Chemistry, 1978 , vol. 43, # 18 p. 3609 - 3611
反应条件
1: AlCl3
2: LiAlH4, TiCl3 / tetrahydrofuran / Heating
View Scheme
参考文献
Baumstark,A.L. et al.
Journal of Organic Chemistry, 1978 , vol. 43, # 18 p. 3609 - 3611
反应条件
formic acid
T=100°C; 96 h;
参考文献
Rio,G.; Bricout,D.
Bulletin de la Societe Chimique de France, 1971 , p. 3557 - 3560
反应条件
1: AlCl3
2: LiAlH4, TiCl3 / tetrahydrofuran / Heating
View Scheme
参考文献
Baumstark,A.L. et al.
Journal of Organic Chemistry, 1978 , vol. 43, # 18 p. 3609 - 3611
反应条件
hydrogenchloride; palladium
Hydrogenation;
参考文献
Weidlich; Meyer-Delius
Chemische Berichte, 1941 , vol. 74, p. 1195,1209
反应条件
potassium tert-butylate
T=240°C; 9 h;
参考文献
Ceylan, Mustafa; Yalcin, Seher; Secen, Hasan; Suetbeyaz, Yasar; Balci, Metin
Journal of Chemical Research - Part S, 2003 , # 1 p. 21 - 23
反应条件
1.1: NaBH4; BF3*OEt2 / tetrahydrofuran / 3 h / 20 °C
1.2: 81 percent / aq. NaOH; H2O2 / 0.5 h / 50 °C
2.1: 80 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / 20 °C
3.1: 97.8 percent / NH2NH2*H2O / 1 h / 90 - 95 °C
4.1: 19.25 percent / I2; Et3N / tetrahydrofuran / 1 h / 20 °C
5.1: 19.25 percent / t-BuOK / 9 h / 240 °C
View Scheme
参考文献
Ceylan, Mustafa; Yalcin, Seher; Secen, Hasan; Suetbeyaz, Yasar; Balci, Metin
Journal of Chemical Research - Part S, 2003 , # 1 p. 21 - 23
