6-乙基-7-羟基-4-甲基-2H-色烯-2-酮合成路线 （共 9 条）
反应条件
trifluoroacetic acid
T=100°C; Pechmann condensation; 0.5 h; Microwave irradiation; regioselective reaction;
参考文献
Zak, Jaroslav; Ron, David; Riva, Elena; Harding, Heather P.; Cross, Benedict C. S.; Baxendale, Ian R.
Chemistry - A European Journal, 2012 , vol. 18, # 32 p. 9901 - 9910
反应条件
sulfuric acid in ethyl acetate
T=20°C; 12 h;
参考文献
Wyatt, Emma E.; Fergus, Suzanne; Galloway, Warren R. J. D.; Bender, Andreas; Fox, David J.; Plowright, Alleyn T.; Jessiman, Alan S.; Welch, Martin; Spring, David R.
Chemical Communications, 2006 , # 31 p. 3296 - 3298
反应条件
hydrogen iodide; acetic anhydride
参考文献
Usgaonkar et al.
Journal of the Indian Chemical Society, 1953 , vol. 30, p. 535,536
反应条件
hydrogenchloride; amalgamated zinc; ethanol
参考文献
Limaye; Limaye
Rasayanam, 1941 , vol. 1, p. 201,205
反应条件
1: amalgamated zinc; aqueous HCl
2: aluminium chloride; nitrobenzene
3: aqueous hydriodic acid; acetic acid anhydride
View Scheme
参考文献
Usgaonkar et al.
Journal of the Indian Chemical Society, 1953 , vol. 30, p. 535,536
反应条件
1: ZnCl2
2: aqueous HCl; amalgamated zinc
3: sulfuric acid
View Scheme
参考文献
Chakravarti; Chakravarty
Journal of the Indian Chemical Society, 1939 , vol. 16, p. 144,147
反应条件
1: aqueous HCl; amalgamated zinc
2: sulfuric acid
View Scheme
参考文献
Chakravarti; Chakravarty
Journal of the Indian Chemical Society, 1939 , vol. 16, p. 144,147
参考文献
Chakravarti; Chakravarty
Journal of the Indian Chemical Society, 1939 , vol. 16, p. 144,147
Full Text Show Details
Desai; Ekhlas
Proceedings - Indian Academy of Sciences, Section A, 1938 , # 8 p. 194,199
Full Text Show Details
Limaye; Limaye
Rasayanam, 1936 , vol. 1, p. 201,204
反应条件
1: 94 percent / 3 h / Heating
2: 76 percent / AlCl3 / 1 h / 170 °C
3: 81 percent / aq. NaOH / 3 h / Heating
View Scheme
参考文献
Limaye; Limaye
Rasayanam, 1941 , vol. 1, p. 201,205
