(S)-(-)-4-苄基氧氮杂环戊烷-2,5-二酮合成路线 (共 17 条)
反应条件
in tetrahydrofuran; toluene T=50°C; 1 h;
参考文献
Sill, Kevin; Vojkovsky, Tomas; Carie, Adam
Patent: US2013/280306 A1, 2013 ;
Location in patent: Paragraph 0392; 0393 ;
反应条件
in tetrahydrofuran T=50°C; Inert atmosphere;
参考文献
Koo, Ahn Na; Lee, Hong Jae; Kim, Sung Eun; Chang, Jeong Ho; Park, Chiyoung; Kim, Chulhee; Park, Jae Hyung; Lee, Sang Cheon
Chemical Communications, 2008 , # 48 p. 6570 - 6572
反应条件
carbon in tetrahydrofuran T=55°C; 0.5 h;
参考文献
Katakai, Ryoichi; Iizuka, Yasuko
Journal of Organic Chemistry, 1985 , vol. 50, # 5 p. 715 - 716
反应条件
phosphorus trichoride in dichloromethane T=0°C; 2 h;
参考文献
Akssira; Boumzebra; Kasmi; Dahdouh; Roumestant; Viallefont
Tetrahedron, 1994 , vol. 50, # 30 p. 9051 - 9060
反应条件
N,N-dimethyl-formamide in dichloromethane T=0 - 20°C;
参考文献
Mobashery, Shahriar; Johnston, Michael
Journal of Organic Chemistry, 1985 , vol. 50, # 12 p. 2200 - 2202
反应条件
phosphorus tribromide in diethyl ether
参考文献
Itoh, Osamu; Honnami, Toshiya; Amano, Akira; Murata, Kouichi; Koichi, Youta; Sugita, Toshio
Journal of Organic Chemistry, 1992 , vol. 57, # 28 p. 7334 - 7338
反应条件
in tetrahydrofuran T=50°C; Inert atmosphere;
参考文献
Li, Yong-Yong; Hua, Shou-Hu; Xiao, Wang; Wang, Hui-Yuan; Luo, Xiao-Hua; Li, Cao; Cheng, Si-Xue; Zhang, Xian-Zheng; Zhuo, Ren-Xi
Journal of Materials Chemistry, 2011 , vol. 21, # 9 p. 3100 - 3106
反应条件
in tetrahydrofuran T=60°C; 4 h;
参考文献
Nagai, Atsushi; Sato, Daisuke; Ishikawa, Junichi; Ochiai, Bungo; Kudo, Hiroto; Endo, Takeshi
Macromolecules, 2004 , vol. 37, # 7 p. 2332 - 2334
反应条件
TEA in tetrahydrofuran T=55 - 60°C;
参考文献
Synthetic Communications, , vol. 31, # 14 p. 2169 - 2175
反应条件
1: 76 percent / aq. NaOH 2: 66.8 percent / PBr3 / diethyl ether View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 28 p. 7334 - 7338