4-(三氯甲基)苯甲酰氯合成路线 （共 16 条）
参考文献
Davies; Perkin
Journal of the Chemical Society, 1922 , vol. 121, p. 2213
反应条件
2-ethoxy-ethanol; lithium tri(t-butoxy)aluminum hydride; carbon dioxide in tetrahydrofuran
T=-65°C; 1 h;
参考文献
Morkved; Cronyn
Journal of Pharmaceutical Sciences, 1982 , vol. 71, # 1 p. 59 - 63
反应条件
1: 99 percent / lithium tri-tert-butoxyaluminum hydride, 2-ethoxyethanol, carbon dioxide / tetrahydrofuran / 1 h / -65 °C
2: 65 percent / p-toluenesulfonic acid / benzene / 3 h / Heating
View Scheme
参考文献
Morkved; Cronyn
Journal of Pharmaceutical Sciences, 1982 , vol. 71, # 1 p. 59 - 63
反应条件
in chloroform; water
参考文献
Dynamit Nobel Aktiengesellschaft
Patent: US4107169 A1, 1978 ;
反应条件
formic acid
T=80 - 85°C;
参考文献
Davies; Perkin
Journal of the Chemical Society, 1922 , vol. 121, p. 2213
参考文献
Davies; Perkin
Journal of the Chemical Society, 1922 , vol. 121, p. 2213
