反应条件
1: triethylamine / chloroform / 0.5 h / Cooling with ice
2: sodium azide / N,N-dimethyl-formamide / 1 h / 80 °C / Inert atmosphere
3: hydrogen / palladium 10 on activated carbon / ethanol / 5 h / 20 °C
View Scheme
参考文献
Kitamura, Takahiro; Yamada, Hajime; Takemura, Shunji; Ashikawa, Masanori; Ishikawa, Tetsuya; Miyake, Yoshiharu; Kouketsu, Akiyasu; Sato, Seiichi; Ishiwata, Hiroyuki; Tabunoki, Yuichiro; Shibasaki, Manabu; Ozawa, Takatoshi; Shigemi, Ryota; Doi, Takeshi; Tamura, Masahiro
Patent: US2011/237590 A1, 2011 ;
US 20110237590 A1
