3-(2-羧醛苯基)丙醛合成路线 (共 11 条)
反应条件
1: With oxygen; ozone in dichloromethane T=-78°C; 0.0833333 h; 2: With poly(ethylene glycol)-triphenylphosphine in dichloromethane T=-78 - 20°C; 2 h;
参考文献
Sieber, Frank; Wentworth Jr., Paul; Janda, Kim D.
Molecules, 2000 , vol. 5, # 8 p. 1018 - 1032
反应条件
iodosylbenzene; Mn(2)2Cl in acetonitrile T=25°C; 48 h; Inert atmosphere;
参考文献
Aghmiz; Mostfa; Iksi; Rivas; Gonzalez; Diaz; El Guemmout; El Laghdach; Echarri; Masdeu-Bulto
Journal of Coordination Chemistry, 2013 , vol. 66, # 14 p. 2567 - 2577
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile T=21°C; 1 h;
参考文献
Mang, Harald; Gross, Johannes; Lara, Miguel; Goessler, Christian; Schoemaker, Hans E.; Guebitz, Georg M.; Kroutil, Wolfgang
Tetrahedron, 2007 , vol. 63, # 16 p. 3350 - 3354
反应条件
water; lithium perchlorate in acetonitrile 3.5 h; Ambient temperatureconstant current electrolysis, -1.3 -1.4 vs SCE, 25 mA/cm2, platimun plate electrode, undivided cell;
参考文献
Maki, Shojiro; Niwa, Haruki; Hirano, Takashi
Synlett, 1997 , # 12 p. 1385 - 1386
反应条件
1: potassium acetate / Behandeln des Reaktionsprodukts mit konz. wss. KOH, zuletzt auf dem Dampfbad 2: lead (IV)-acetate; benzene View Scheme
参考文献
Blount
Journal of the Chemical Society, 1933 , p. 553
反应条件
lead(IV) acetate; benzene
参考文献
Blount
Journal of the Chemical Society, 1933 , p. 553
反应条件
in xylene T=60°C; ΔH(excit.), ΔS(excit.); Rate constantThermodynamic dataQuantum yield;
参考文献
Baumstark, Alfons L.; Vasquez, Pedro C.
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5213 - 5216
参考文献
v. Braun; Zobel
Chemische Berichte, 1923 , vol. 56, p. 2148
反应条件
permanganate(VII) ion; sodium carbonate
参考文献
v. Braun; Zobel
Chemische Berichte, 1923 , vol. 56, p. 2148
反应条件
diethyl ether; aluminium amalgam
参考文献
NOVARTIS AG; NOVARTIS PHARMA GMBH
Patent: WO2005/51911 A1, 2005 ;
Location in patent: Page/Page column 72 ;
WO 2005/051911 A1