4,4,5,5,5-五氟戊醇合成路线 （共 17 条）
反应条件
hydrogen; triethylamine; platinum(IV) oxide in ethyl acetate T=25°C; 3 h;
参考文献
Li, Xun; Provencher, Louis; Singh, Shankar M.
Tetrahedron Letters, 1994 , vol. 35, # 49 p. 9141 - 9144
反应条件
triethylamine; palladium in water; ethyl acetate
反应条件
hydrogen; triethylamine; palladium
反应条件
sodium hydroxide 1 h; Heating;
参考文献
Larsson, Ulf; Carlson, Rolf; Leroy, Jacques
Acta Chemica Scandinavica, 1993 , vol. 47, # 4 p. 380 - 390
反应条件
1: 78 percent / azoisobutyronitrile (AIBN), Bu3SnH / 55 - 65 °C 2: 92 percent / aq. NaOH / 1 h / Heating View Scheme
参考文献
Acta Chemica Scandinavica, , vol. 47, # 4 p. 380 - 390
反应条件
Jone's reagent in acetone T=0 - 20°C; 1 h;
参考文献
US6645951 B1, ;
Page/Page column 281 ;
反应条件
potassium permanganate in water T=65 - 70°C;
参考文献
Organic Process Research and Development, , vol. 3, # 5 p. 363 - 364
反应条件
1: triethylamine / acetonitrile / 2 h / 20 °C / Inert atmosphere; Large scale reaction 2: sodium hydroxide / water; acetonitrile / 83 h / 40 - 72 °C / Inert atmosphere; Large scale reaction 3: bromine; triphenylphosphine / acetonitrile / 3 h / 23 °C / Large scale reaction View Scheme
参考文献
Organic Process Research and Development, , vol. 14, # 3 p. 544 - 552
反应条件
1: triethylamine / acetonitrile / 2 h / 20 °C / Inert atmosphere; Large scale reaction 2: sodium hydroxide / water; acetonitrile / 83 h / 40 - 72 °C / Inert atmosphere; Large scale reaction View Scheme
参考文献
Organic Process Research and Development, , vol. 14, # 3 p. 544 - 552
