4,5-二羟基-3,6-双[(4-甲基-2-磺基苯基)偶氮]-2,7-萘磺酸合成路线 （共 3 条）
反应条件
sulfur dioxide; potassium iodide in hydrogenchloride dissolving educt in 6M HCl; bubbling of SO2; extn. with ether, evapn.;
参考文献
Bruker, A. B.
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2282 - 2284
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2223 - 2226
Full Text Show Details
Gmelin Handbook: Sb: Org.Comp.2, 1.3.1.1.2.3.3, page 103 - 112
反应条件
in diethyl ether 6 h; Inert atmosphere;
参考文献
Singhal, Kiran; Chaudhary, Subhas Kumar; Prakash, Om
Asian Journal of Chemistry, 2013 , vol. 25, # 16 p. 9020 - 9022
反应条件
in neat (no solvent) a 1:2 molar mixt. of Ar3Sb and SbCl3 was kept at ca.35°C overnight; satisfactory elem. anal. and IR spectrum;
参考文献
Nunn, Michael; Sowerby, D. Bryan; Wesolek, Denise M.
Journal of Organometallic Chemistry, 1983 , vol. 251, # 3 p. C45 - C46
