5-Hydroxy-3,6,7-三甲氧基-2-(4-甲氧基苯基)色烯-4-酮合成路线 (共 7 条)
反应条件
aluminum tri-bromide in acetonitrile 2 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 52, # 21 p. 4702 - 4709
反应条件
sodium 4-methoxyphenylacetate T=180°C; P=20 Torr; Erwaermen des Reaktionsprodukts mit wss.-aethanol. Kalilauge;
参考文献
Journal of the Chemical Society, , p. 46,47
反应条件
1: 1.) potassium benzoate, 2.) K2CO3 / 1.) 170/180 deg C, 8 h, 2.) acetone, reflux, 2.5-4 h 2: 93 percent / AlBr3 / acetonitrile / 0.33 h / 0 - 5 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 37, # 5 p. 1216 - 1220
反应条件
1: 1.) potassium benzoate, 2.) K2CO3 / 1.) 170/180 deg C, 8 h, 2.) acetone, reflux, 2.5-4 h 2: 93 percent / AlBr3 / acetonitrile / 0.33 h / 0 - 5 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 37, # 5 p. 1216 - 1220
反应条件
methanol; diethyl ether
参考文献
Proceedings - Indian Academy of Sciences, Section A, , # 49 p. 241,247
反应条件
hydrogen iodide; phenol
T=140°C;
参考文献
Goldsworthy; Robinson
Journal of the Chemical Society, 1937 , p. 46,47
反应条件
sodium hydroxide; acetone
参考文献
Goldsworthy; Robinson
Journal of the Chemical Society, 1937 , p. 46,47