1-(2,4-二氯苯基)乙醇合成路线 (共 15 条)
反应条件
sodium borohydride in methanol; water
参考文献
TAKEDA PHARMACEUTICAL COMPANY LIMITED
Patent: WO2006/57448 A1, 2006 ;
Location in patent: Page/Page column 116-117 ;
反应条件
diphosphorous tetraiodide; tetraethylammonium bromide; water in dichloromethane T=20°C; 6 h; regioselective reaction;
参考文献
Telvekar, Vikas N.; Rane, Rajesh A.
Synthetic Communications, 2010 , vol. 40, # 14 p. 2108 - 2112
反应条件
1: AlCl3 / 100 °C 2: isopropyl alcohol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 68, p. 861,863
Industrial and Engineering Chemistry, , vol. 39, p. 1486,1487
参考文献
Journal of the American Chemical Society, , vol. 68, p. 861,863
Industrial and Engineering Chemistry, , vol. 39, p. 1486,1487
参考文献
Journal of the Chemical Society, , p. 1165
参考文献
Journal of the Chemical Society, , p. 1165
反应条件
nachfolgende Behandlung mit Acetaldehyd;
参考文献
Journal of the Chemical Society, , p. 1165
反应条件
hydrogenchloride; 3-chloro-benzenecarboperoxoic acid in N,N-dimethyl-formamide T=25°C; 6 h;
参考文献
Kim, Hak Jin; Kim, Hyoung Rae; Ryu, Eung K.
Synthetic Communications, 1990 , vol. 20, # 11 p. 1625 - 1629
参考文献
Evans; Mabbott; Turner
Journal of the Chemical Society, 1927 , p. 1165
反应条件
aluminum oxide T=350 - 400°C;
参考文献
Koton et al.
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 489; engl. Ausg. S. 551